Abstract
The construction of high signal-to-noise, artefact-free secondary electron images in the elevated pressure conditions of an environmental SEM is a nontrivial process. The interactions of information carrying species, as well as probe beam electrons, with the chamber gas are the major reasons for such complications. In this paper, we discuss and review the present understanding of these phenomena. In addition, we outline procedures for assessing the signal-amplifying and charge-neutralising capabilities of an environmental gas. It is only with a knowledge of such parameters and an appreciation of the gas-electron collision processes that one can optimise the microscope's operating parameters. Moreover, such information enables the separation of topographic detail from artefactual features in the detected electron images.
| Original language | English |
|---|---|
| Pages (from-to) | 467-473 |
| Number of pages | 7 |
| Journal | Scanning |
| Volume | 18 |
| Issue number | 7 |
| DOIs | |
| State | Published - Oct 1996 |
Keywords
- Amplification
- Charge suppression
- Electron-gas interactions
- Environmental scanning electron microscope
- Gaseous detection
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