Fabrication and characterization of molybdenum oxide nanofibers by electrospinning

Guan Wang; Xianrong Huang; Michael Dudley; Pelagia Irene Gouma; Xiaoqing Yang

doi:10.1557/proc-0900-o03-22

Fabrication and characterization of molybdenum oxide nanofibers by electrospinning

Guan Wang
, Xianrong Huang
, Michael Dudley
, Pelagia Irene Gouma
, Xiaoqing Yang

Materials Science and Engineering

Stony Brook University

Stony Brook University
Brookhaven National Laboratory

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

2 Scopus citations

Abstract

Molybdenum oxide/ Poly (ethylene oxide) composite nanofibers were prepared by combining the sol-gel process and electrspinning technique. An ethanol solution of Poly(ethylene oxide) (PEO) was mixed with molybdenum isopropoxide to form a precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure molybdenum oxide nanofibers and nano-rods were obtained with diameters of 100-nanometer scale. Morphology of the fibers has been characterized by scanning electric microscopy. Components and structures of the final products have been identified by EDAX and grazing incidence XRD. Calcination process has been studied by DSC and TG analysis. The real time dynamics of the structural evolution from composite fibers to nanocrystalline metal oxide fibers has been investigated by synchrotron-based in-situ x-ray diffraction.

Original language	English
Title of host publication	Nanoparticles and Nanostructures in Sensors and Catalysis
Publisher	Materials Research Society
Pages	81-86
Number of pages	6
ISBN (Print)	1558998543, 9781558998544
DOIs	https://doi.org/10.1557/proc-0900-o03-22
State	Published - 2005
Event	2005 MRS Fall Meeting - Boston, MA, United States Duration: Nov 28 2005 → Dec 2 2005

Publication series

Name	Materials Research Society Symposium Proceedings
Volume	900

Conference

Conference	2005 MRS Fall Meeting
Country/Territory	United States
City	Boston, MA
Period	11/28/05 → 12/2/05

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10.1557/proc-0900-o03-22

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@inproceedings{52c13b9424bf41628ee5f3ff27b0491c,

title = "Fabrication and characterization of molybdenum oxide nanofibers by electrospinning",

abstract = "Molybdenum oxide/ Poly (ethylene oxide) composite nanofibers were prepared by combining the sol-gel process and electrspinning technique. An ethanol solution of Poly(ethylene oxide) (PEO) was mixed with molybdenum isopropoxide to form a precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure molybdenum oxide nanofibers and nano-rods were obtained with diameters of 100-nanometer scale. Morphology of the fibers has been characterized by scanning electric microscopy. Components and structures of the final products have been identified by EDAX and grazing incidence XRD. Calcination process has been studied by DSC and TG analysis. The real time dynamics of the structural evolution from composite fibers to nanocrystalline metal oxide fibers has been investigated by synchrotron-based in-situ x-ray diffraction.",

author = "Guan Wang and Xianrong Huang and Michael Dudley and Gouma, \{Pelagia Irene\} and Xiaoqing Yang",

year = "2005",

doi = "10.1557/proc-0900-o03-22",

language = "English",

isbn = "1558998543",

series = "Materials Research Society Symposium Proceedings",

publisher = "Materials Research Society",

pages = "81--86",

booktitle = "Nanoparticles and Nanostructures in Sensors and Catalysis",

note = "2005 MRS Fall Meeting ; Conference date: 28-11-2005 Through 02-12-2005",

}

Wang, G, Huang, X, Dudley, M, Gouma, PI & Yang, X 2005, Fabrication and characterization of molybdenum oxide nanofibers by electrospinning. in Nanoparticles and Nanostructures in Sensors and Catalysis. Materials Research Society Symposium Proceedings, vol. 900, Materials Research Society, pp. 81-86, 2005 MRS Fall Meeting, Boston, MA, United States, 11/28/05. https://doi.org/10.1557/proc-0900-o03-22

Fabrication and characterization of molybdenum oxide nanofibers by electrospinning. / Wang, Guan; Huang, Xianrong; Dudley, Michael et al.
Nanoparticles and Nanostructures in Sensors and Catalysis. Materials Research Society, 2005. p. 81-86 (Materials Research Society Symposium Proceedings; Vol. 900).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Fabrication and characterization of molybdenum oxide nanofibers by electrospinning

AU - Wang, Guan

AU - Huang, Xianrong

AU - Dudley, Michael

AU - Gouma, Pelagia Irene

AU - Yang, Xiaoqing

PY - 2005

Y1 - 2005

N2 - Molybdenum oxide/ Poly (ethylene oxide) composite nanofibers were prepared by combining the sol-gel process and electrspinning technique. An ethanol solution of Poly(ethylene oxide) (PEO) was mixed with molybdenum isopropoxide to form a precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure molybdenum oxide nanofibers and nano-rods were obtained with diameters of 100-nanometer scale. Morphology of the fibers has been characterized by scanning electric microscopy. Components and structures of the final products have been identified by EDAX and grazing incidence XRD. Calcination process has been studied by DSC and TG analysis. The real time dynamics of the structural evolution from composite fibers to nanocrystalline metal oxide fibers has been investigated by synchrotron-based in-situ x-ray diffraction.

AB - Molybdenum oxide/ Poly (ethylene oxide) composite nanofibers were prepared by combining the sol-gel process and electrspinning technique. An ethanol solution of Poly(ethylene oxide) (PEO) was mixed with molybdenum isopropoxide to form a precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure molybdenum oxide nanofibers and nano-rods were obtained with diameters of 100-nanometer scale. Morphology of the fibers has been characterized by scanning electric microscopy. Components and structures of the final products have been identified by EDAX and grazing incidence XRD. Calcination process has been studied by DSC and TG analysis. The real time dynamics of the structural evolution from composite fibers to nanocrystalline metal oxide fibers has been investigated by synchrotron-based in-situ x-ray diffraction.

UR - https://www.scopus.com/pages/publications/34249931252

U2 - 10.1557/proc-0900-o03-22

DO - 10.1557/proc-0900-o03-22

M3 - Conference contribution

SN - 1558998543

SN - 9781558998544

T3 - Materials Research Society Symposium Proceedings

SP - 81

EP - 86

BT - Nanoparticles and Nanostructures in Sensors and Catalysis

PB - Materials Research Society

T2 - 2005 MRS Fall Meeting

Y2 - 28 November 2005 through 2 December 2005

ER -

Fabrication and characterization of molybdenum oxide nanofibers by electrospinning

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