High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements

Tadanori Koga; Shuiqin Zhou; Benjamin Chu; John L. Fulton; Shu Yang; Christopher K. Ober; Burak Erman

doi:10.1063/1.1372696

High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements

Tadanori Koga
, Shuiqin Zhou
, Benjamin Chu
, John L. Fulton
, Shu Yang
, Christopher K. Ober
, Burak Erman

Materials Science and Engineering

Stony Brook University

Stony Brook University
Pacific Northwest National Laboratory
Cornell University
Sabanci University

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

A cell for in situ observation of self-assembled nanostructured materials in high-pressure fluids, including supercritical carbon dioxide, has been constructed and tested. The compact cell can be used for simultaneous small-angle x-ray scattering, laser light scattering, visual observation, and some other types of spectroscopic measurements. The light scattering plane is normal to the x-ray scattering plane with the optical axis and the x-ray axis being perpendicular to each other. The scattering is detected at the intersection of the light and x-ray beams, and thus one effectively probes the same scattering volume. Some preliminary experimental results for the micellar self-assembly of a fluorinated block copolymer in supercritical carbon dioxide are presented.

Original language	English
Pages (from-to)	2679-2685
Number of pages	7
Journal	Review of Scientific Instruments
Volume	72
Issue number	6
DOIs	https://doi.org/10.1063/1.1372696
State	Published - Jun 2001

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10.1063/1.1372696

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title = "High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements",

abstract = "A cell for in situ observation of self-assembled nanostructured materials in high-pressure fluids, including supercritical carbon dioxide, has been constructed and tested. The compact cell can be used for simultaneous small-angle x-ray scattering, laser light scattering, visual observation, and some other types of spectroscopic measurements. The light scattering plane is normal to the x-ray scattering plane with the optical axis and the x-ray axis being perpendicular to each other. The scattering is detected at the intersection of the light and x-ray beams, and thus one effectively probes the same scattering volume. Some preliminary experimental results for the micellar self-assembly of a fluorinated block copolymer in supercritical carbon dioxide are presented.",

author = "Tadanori Koga and Shuiqin Zhou and Benjamin Chu and Fulton, \{John L.\} and Shu Yang and Ober, \{Christopher K.\} and Burak Erman",

year = "2001",

month = jun,

doi = "10.1063/1.1372696",

language = "English",

volume = "72",

pages = "2679--2685",

journal = "Review of Scientific Instruments",

issn = "0034-6748",

publisher = "American Institute of Physics",

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T1 - High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements

AU - Koga, Tadanori

AU - Zhou, Shuiqin

AU - Chu, Benjamin

AU - Fulton, John L.

AU - Yang, Shu

AU - Ober, Christopher K.

AU - Erman, Burak

PY - 2001/6

Y1 - 2001/6

N2 - A cell for in situ observation of self-assembled nanostructured materials in high-pressure fluids, including supercritical carbon dioxide, has been constructed and tested. The compact cell can be used for simultaneous small-angle x-ray scattering, laser light scattering, visual observation, and some other types of spectroscopic measurements. The light scattering plane is normal to the x-ray scattering plane with the optical axis and the x-ray axis being perpendicular to each other. The scattering is detected at the intersection of the light and x-ray beams, and thus one effectively probes the same scattering volume. Some preliminary experimental results for the micellar self-assembly of a fluorinated block copolymer in supercritical carbon dioxide are presented.

AB - A cell for in situ observation of self-assembled nanostructured materials in high-pressure fluids, including supercritical carbon dioxide, has been constructed and tested. The compact cell can be used for simultaneous small-angle x-ray scattering, laser light scattering, visual observation, and some other types of spectroscopic measurements. The light scattering plane is normal to the x-ray scattering plane with the optical axis and the x-ray axis being perpendicular to each other. The scattering is detected at the intersection of the light and x-ray beams, and thus one effectively probes the same scattering volume. Some preliminary experimental results for the micellar self-assembly of a fluorinated block copolymer in supercritical carbon dioxide are presented.

UR - https://www.scopus.com/pages/publications/0035362316

U2 - 10.1063/1.1372696

DO - 10.1063/1.1372696

M3 - Article

SN - 0034-6748

VL - 72

SP - 2679

EP - 2685

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

IS - 6

ER -

High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements

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