Theory of combined TOSS-multiple-pulse-scaling experiments

D. P. Raleigh; E. T. Olejniczak; R. G. Griffin

doi:10.1016/0022-2364(91)90076-6

Theory of combined TOSS-multiple-pulse-scaling experiments

D. P. Raleigh
, E. T. Olejniczak
, R. G. Griffin

Chemistry

Stony Brook University

Massachusetts Institute of Technology

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

The theory of hybrid experiments which combine TOSS-type sequences with multiple-pulse-scaling sequences to efficiently eliminate rotational sidebands is described. The analysis relies on the magnetization vector model of magic-angle spinning NMR and leads to a simple derivation of the equations which govern the experiments. New pulse sequences are given for a wide range of experimental conditions.

Original language	English
Pages (from-to)	472-484
Number of pages	13
Journal	Journal of Magnetic Resonance (1969)
Volume	93
Issue number	3
DOIs	https://doi.org/10.1016/0022-2364(91)90076-6
State	Published - Jul 1991

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title = "Theory of combined TOSS-multiple-pulse-scaling experiments",

abstract = "The theory of hybrid experiments which combine TOSS-type sequences with multiple-pulse-scaling sequences to efficiently eliminate rotational sidebands is described. The analysis relies on the magnetization vector model of magic-angle spinning NMR and leads to a simple derivation of the equations which govern the experiments. New pulse sequences are given for a wide range of experimental conditions.",

author = "Raleigh, \{D. P.\} and Olejniczak, \{E. T.\} and Griffin, \{R. G.\}",

year = "1991",

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AU - Raleigh, D. P.

AU - Olejniczak, E. T.

AU - Griffin, R. G.

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Y1 - 1991/7

N2 - The theory of hybrid experiments which combine TOSS-type sequences with multiple-pulse-scaling sequences to efficiently eliminate rotational sidebands is described. The analysis relies on the magnetization vector model of magic-angle spinning NMR and leads to a simple derivation of the equations which govern the experiments. New pulse sequences are given for a wide range of experimental conditions.

AB - The theory of hybrid experiments which combine TOSS-type sequences with multiple-pulse-scaling sequences to efficiently eliminate rotational sidebands is described. The analysis relies on the magnetization vector model of magic-angle spinning NMR and leads to a simple derivation of the equations which govern the experiments. New pulse sequences are given for a wide range of experimental conditions.

UR - https://www.scopus.com/pages/publications/0346149303

U2 - 10.1016/0022-2364(91)90076-6

DO - 10.1016/0022-2364(91)90076-6

M3 - Article

SN - 0022-2364

VL - 93

SP - 472

EP - 484

JO - Journal of Magnetic Resonance (1969)

JF - Journal of Magnetic Resonance (1969)

IS - 3

ER -

Theory of combined TOSS-multiple-pulse-scaling experiments

Abstract

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